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Information card for entry 7704679
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Coordinates | 7704679.cif |
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Original paper (by DOI) | HTML |
Formula | C48 H52 Fe P4 Si |
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Calculated formula | C48 H52 Fe P4 Si |
Title of publication | Pyridine N-oxide promoted hydrosilylation of carbonyl compounds catalyzed by [PSiP]-pincer iron hydrides. |
Authors of publication | Chang, Guoliang; Zhang, Peng; Yang, Wenjing; Xie, Shangqing; Sun, Hongjian; Li, Xiaoyan; Fuhr, Olaf; Fenske, Dieter |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2020 |
Journal volume | 49 |
Journal issue | 27 |
Pages of publication | 9349 - 9354 |
a | 18.4493 ± 0.0002 Å |
b | 21.2072 ± 0.0002 Å |
c | 10.7787 ± 0.0003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 4217.25 ± 0.13 Å3 |
Cell temperature | 180 K |
Ambient diffraction temperature | 180 K |
Number of distinct elements | 5 |
Space group number | 62 |
Hermann-Mauguin space group symbol | P n m a |
Hall space group symbol | -P 2ac 2n |
Residual factor for all reflections | 0.0326 |
Residual factor for significantly intense reflections | 0.0282 |
Weighted residual factors for significantly intense reflections | 0.0764 |
Weighted residual factors for all reflections included in the refinement | 0.0789 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.049 |
Diffraction radiation wavelength | 1.34143 Å |
Diffraction radiation type | GaKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7704679.html
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