Information card for entry 7704711

Structure parameters

• Formula: C47 H33 Al F36 Ge N O4 P
• Calculated formula: C47 H33 Al F36 Ge N O4 P
• Title of publication: Cooperative N-H bond activation by amido-Ge(ii) cations.
• Authors of publication: Zhou, Xueer; Vasko, Petra; Hicks, Jamie; Fuentes, M Ángeles; Heilmann, Andreas; Kolychev, Eugene L.; Aldridge, Simon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 27
• Pages of publication: 9495 - 9504
• a: 12.1911 ± 0.0003 Å
• b: 15.3762 ± 0.0006 Å
• c: 29.9659 ± 0.001 Å
• α: 83.214 ± 0.003°
• β: 88.694 ± 0.002°
• γ: 87.381 ± 0.002°
• Cell volume: 5571.2 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0798
• Residual factor for significantly intense reflections: 0.0647
• Weighted residual factors for significantly intense reflections: 0.1707
• Weighted residual factors for all reflections included in the refinement: 0.1824
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No