Information card for entry 7704714

Structure parameters

• Formula: C52 H52 Al Br F36 Ge2 N6 O4
• Calculated formula: C52 H52 Al Br F36 Ge2 N6 O4
• Title of publication: Cooperative N-H bond activation by amido-Ge(ii) cations.
• Authors of publication: Zhou, Xueer; Vasko, Petra; Hicks, Jamie; Fuentes, M Ángeles; Heilmann, Andreas; Kolychev, Eugene L.; Aldridge, Simon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 27
• Pages of publication: 9495 - 9504
• a: 11.0633 ± 0.0001 Å
• b: 18.7791 ± 0.0002 Å
• c: 18.8201 ± 0.0002 Å
• α: 61.968 ± 0.001°
• β: 80.519 ± 0.001°
• γ: 80.424 ± 0.001°
• Cell volume: 3386.38 ± 0.07 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0293
• Residual factor for significantly intense reflections: 0.0265
• Weighted residual factors for significantly intense reflections: 0.0662
• Weighted residual factors for all reflections included in the refinement: 0.0681
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No