Information card for entry 7704746

Structure parameters

• Formula: C23 H19 Cl N O P
• Calculated formula: C23 H19 Cl N O P
• Title of publication: (2-Pyridyloxy)arsines as ligands in transition metal chemistry: a stepwise As(iii) →As(ii) →As(i) reduction.
• Authors of publication: Gericke, Robert; Wagler, Jörg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 29
• Pages of publication: 10042 - 10051
• a: 9.3905 ± 0.0002 Å
• b: 9.3905 ± 0.0002 Å
• c: 40.1802 ± 0.0017 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3068.46 ± 0.16 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 169
• Hermann-Mauguin space group symbol: P 61
• Hall space group symbol: P 61
• Residual factor for all reflections: 0.0362
• Residual factor for significantly intense reflections: 0.0325
• Weighted residual factors for significantly intense reflections: 0.0761
• Weighted residual factors for all reflections included in the refinement: 0.0806
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No