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Information card for entry 7704759
Preview
Coordinates | 7704759.cif |
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Original paper (by DOI) | HTML |
Formula | C45 H111 Fe Li O6 P6 Si3 |
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Calculated formula | C33 H81 Fe P6 Si3 |
Title of publication | Homoleptic mono-, di-, and tetra-iron complexes featuring phosphido ligands: a synthetic, structural, and spectroscopic study. |
Authors of publication | Kaniewska, Kinga; Ponikiewski, Łukasz; Szynkiewicz, Natalia; Cieślik, Bartłomiej; Pikies, Jerzy; Krzystek, J.; Dragulescu-Andrasi, Alina; Stoian, Sebastian A.; Grubba, Rafał |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2020 |
Journal volume | 49 |
Journal issue | 29 |
Pages of publication | 10091 - 10103 |
a | 17.6278 ± 0.0006 Å |
b | 17.5183 ± 0.0007 Å |
c | 24.0113 ± 0.0008 Å |
α | 90° |
β | 94.002 ± 0.003° |
γ | 90° |
Cell volume | 7396.8 ± 0.5 Å3 |
Cell temperature | 121 ± 2 K |
Ambient diffraction temperature | 121 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1346 |
Residual factor for significantly intense reflections | 0.0911 |
Weighted residual factors for significantly intense reflections | 0.2325 |
Weighted residual factors for all reflections included in the refinement | 0.2647 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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