Information card for entry 7704765

Structure parameters

• Formula: C30 H82 Mn2 P10
• Calculated formula: C30 H80.8428 Mn2 P10
• Title of publication: Reactions of [(dmpe)₂MnH(C₂H₄)]: synthesis and characterization of manganese(i) borohydride and hydride complexes.
• Authors of publication: Price, Jeffrey S.; DeJordy, Declan M.; Emslie, David J. H.; Britten, James F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 29
• Pages of publication: 9983 - 9994
• a: 15.392 ± 0.002 Å
• b: 10.4309 ± 0.0014 Å
• c: 28.529 ± 0.004 Å
• α: 90°
• β: 98.652 ± 0.002°
• γ: 90°
• Cell volume: 4528.3 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1648
• Residual factor for significantly intense reflections: 0.1092
• Weighted residual factors for significantly intense reflections: 0.2817
• Weighted residual factors for all reflections included in the refinement: 0.3234
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No