Information card for entry 7704823

Structure parameters

• Formula: C24 H39 Cu N8 O11 V4
• Calculated formula: C24 H39 Cu N8 O11 V4
• Title of publication: Imidazole-directed fabrication of three polyoxovanadate-based copper frameworks as efficient catalysts for constructing C-N bonds.
• Authors of publication: Huang, Xianqiang; Qi, Yuquan; Gu, Yuxiao; Gong, Shuwen; Shen, Guodong; Li, Qiang; Li, Jikun
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 31
• Pages of publication: 10970 - 10976
• a: 11.2508 ± 0.0008 Å
• b: 11.9199 ± 0.0009 Å
• c: 15.2277 ± 0.0014 Å
• α: 105.431 ± 0.002°
• β: 94.168 ± 0.001°
• γ: 108.872 ± 0.002°
• Cell volume: 1834.3 ± 0.3 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0878
• Residual factor for significantly intense reflections: 0.0611
• Weighted residual factors for significantly intense reflections: 0.1762
• Weighted residual factors for all reflections included in the refinement: 0.1938
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No