Information card for entry 7704971

Structure parameters

• Formula: C62.15 H100 Ca N3 O1.35 Si3 Sn
• Calculated formula: C59 H93 Ca N3 O Si3 Sn
• Title of publication: A versatile nitrogen ligand for alkaline-earth chemistry.
• Authors of publication: Chapple, Peter M.; Cordier, Marie; Dorcet, Vincent; Roisnel, Thierry; Carpentier, Jean-François; Sarazin, Yann
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 34
• Pages of publication: 11878 - 11889
• a: 13.0735 ± 0.0018 Å
• b: 20.434 ± 0.002 Å
• c: 25.973 ± 0.003 Å
• α: 90°
• β: 91.784 ± 0.005°
• γ: 90°
• Cell volume: 6935.2 ± 1.4 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0913
• Residual factor for significantly intense reflections: 0.0563
• Weighted residual factors for significantly intense reflections: 0.1304
• Weighted residual factors for all reflections included in the refinement: 0.1493
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No