Information card for entry 7705030

Structure parameters

• Formula: C168 H145 Mg2 N5 O0.25
• Calculated formula: C148 H123.522 Mg2 N4 O0.478
• Title of publication: Magnesium hydrides bearing sterically demanding amidinate ligands: synthesis, reactivity and catalytic application.
• Authors of publication: Bakewell, Clare
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 32
• Pages of publication: 11354 - 11360
• a: 23.3074 ± 0.0003 Å
• b: 23.7367 ± 0.0002 Å
• c: 24.8704 ± 0.0003 Å
• α: 90°
• β: 111.768 ± 0.001°
• γ: 90°
• Cell volume: 12778.2 ± 0.3 ų
• Cell temperature: 154.4 ± 0.8 K
• Ambient diffraction temperature: 154.4 ± 0.8 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0693
• Residual factor for significantly intense reflections: 0.0538
• Weighted residual factors for significantly intense reflections: 0.1404
• Weighted residual factors for all reflections included in the refinement: 0.1527
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No