Information card for entry 7705088

Structure parameters

• Formula: C62 H96 O5 S4 Si2
• Calculated formula: C62 H96 O5 S4 Si2
• Title of publication: Synthesis and structures of diaryloxystannylenes and -plumbylenes embedded in 1,3-diethers of thiacalix[4]arene.
• Authors of publication: Kuriki, Ryunosuke; Kuwabara, Takuya; Ishii, Youichi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 35
• Pages of publication: 12234 - 12241
• a: 13.51 ± 0.002 Å
• b: 15.106 ± 0.002 Å
• c: 16.04 ± 0.002 Å
• α: 79.593 ± 0.005°
• β: 81.074 ± 0.004°
• γ: 89.23 ± 0.006°
• Cell volume: 3180.3 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0862
• Residual factor for significantly intense reflections: 0.0598
• Weighted residual factors for significantly intense reflections: 0.1317
• Weighted residual factors for all reflections included in the refinement: 0.1488
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No