Information card for entry 7705163

Structure parameters

• Formula: C30 H46 Br0.84 Cl3.16 Mn N4 Si2
• Calculated formula: C30 H46 Br0.84 Cl3.16 Mn N4 Si2
• Title of publication: Aminolysis of bis[bis(trimethylsilyl)amido]-manganese, -iron, and -cobalt for the synthesis of mono- and bis-silylene complexes.
• Authors of publication: He, Zhiyuan; Xue, Xiaolian; Liu, Yilan; Yu, Na; Krogman, Jeremy P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 36
• Pages of publication: 12586 - 12591
• a: 10.5954 ± 0.0009 Å
• b: 10.9184 ± 0.0008 Å
• c: 17.2222 ± 0.0014 Å
• α: 77.08 ± 0.004°
• β: 79.212 ± 0.004°
• γ: 73.855 ± 0.004°
• Cell volume: 1848.6 ± 0.3 ų
• Cell temperature: 150.03 K
• Ambient diffraction temperature: 150.03 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0916
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for significantly intense reflections: 0.0936
• Weighted residual factors for all reflections included in the refinement: 0.1096
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No