Information card for entry 7705354

Structure parameters

• Formula: C55 H78 B Cl Ga N4 O Sb
• Calculated formula: C55 H78 B Cl Ga N4 O Sb
• Title of publication: Synthesis of heteroleptic gallium-substituted antimony hydrides by stepwise β-H elimination.
• Authors of publication: Helling, Christoph; Wölper, Christoph; Schulz, Stephan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 34
• Pages of publication: 11835 - 11842
• a: 19.112 ± 0.003 Å
• b: 13.617 ± 0.002 Å
• c: 21.17 ± 0.004 Å
• α: 90°
• β: 99.737 ± 0.003°
• γ: 90°
• Cell volume: 5430.1 ± 1.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0639
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.069
• Weighted residual factors for all reflections included in the refinement: 0.0782
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No