Information card for entry 7705403

Structure parameters

• Formula: C84 H117 Cu2 N6 P7 Si
• Calculated formula: C84 H117 Cu2 N6 P7 Si
• Title of publication: Incorporation of coinage metal-NHC complexes into heptaphosphide clusters.
• Authors of publication: Jo, Minyoung; Li, Jingbai; Dragulescu-Andrasi, Alina; Rogachev, Andrey Yu; Shatruk, Michael
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 37
• Pages of publication: 12955 - 12959
• a: 24.29 ± 0.002 Å
• b: 25.025 ± 0.002 Å
• c: 28.319 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 17214 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 6
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.1389
• Residual factor for significantly intense reflections: 0.0882
• Weighted residual factors for significantly intense reflections: 0.2103
• Weighted residual factors for all reflections included in the refinement: 0.2456
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No