Information card for entry 7705444

Structure parameters

• Formula: C68 H74 B F12 N2 O Si3
• Calculated formula: C68 H74 B F12 N2 O Si3
• Title of publication: An intermolecular FLP System derived from an NHC-coordinated trisilacyclopropylidene.
• Authors of publication: Guddorf, Benedikt J.; Hepp, Alexander; Daniliuc, Constantin; Stephan, Douglas W.; Lips, Felicitas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 38
• Pages of publication: 13386 - 13392
• a: 12.0609 ± 0.0007 Å
• b: 12.8451 ± 0.0009 Å
• c: 22.3125 ± 0.0014 Å
• α: 85.936 ± 0.002°
• β: 75.667 ± 0.002°
• γ: 84.697 ± 0.002°
• Cell volume: 3330.7 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1246
• Residual factor for significantly intense reflections: 0.0812
• Weighted residual factors for significantly intense reflections: 0.1482
• Weighted residual factors for all reflections included in the refinement: 0.1652
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No