Information card for entry 7705569

Structure parameters

• Formula: C27 H18 F36 K2 O9 Sn
• Calculated formula: C27 H18 F36 K2 O9 Sn
• Title of publication: Formation of monomeric Sn(ii) and Sn(iv) perfluoropinacolate complexes and their characterization by ¹¹⁹Sn Mössbauer and ¹¹⁹Sn NMR spectroscopies.
• Authors of publication: Elinburg, Jessica K.; Hyre, Ariel S.; McNeely, James; Alam, Todd M.; Klenner, Steffen; Pöttgen, Rainer; Rheingold, Arnold L.; Doerrer, Linda H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 39
• Pages of publication: 13773 - 13785
• a: 10.869 ± 0.002 Å
• b: 18.441 ± 0.004 Å
• c: 21.954 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4400.4 ± 1.5 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 56
• Hermann-Mauguin space group symbol: P c c n
• Hall space group symbol: -P 2ab 2ac
• Residual factor for all reflections: 0.0715
• Residual factor for significantly intense reflections: 0.053
• Weighted residual factors for significantly intense reflections: 0.0921
• Weighted residual factors for all reflections included in the refinement: 0.0969
• Goodness-of-fit parameter for all reflections included in the refinement: 1.268
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No