Information card for entry 7705669

Structure parameters

• Formula: C2 H129 As4 K17 Na2 O204 Sm2 W38
• Calculated formula: C2 As4 K17 Na2 O204 Sm2 W38
• Title of publication: H-shaped oxalate-bridging lanthanoid-incorporated arsenotungstates.
• Authors of publication: Chen, Hanhan; Xiao, Zikang; Yan, Bing; Wu, Hechen; Ma, Pengtao; Wang, Jingping; Niu, Jingyang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 44
• Pages of publication: 15731 - 15738
• a: 12.2892 ± 0.0005 Å
• b: 18.5454 ± 0.0009 Å
• c: 22.9794 ± 0.0011 Å
• α: 67.218 ± 0.002°
• β: 81.116 ± 0.002°
• γ: 79.915 ± 0.002°
• Cell volume: 4732.3 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 149.98 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0645
• Residual factor for significantly intense reflections: 0.0533
• Weighted residual factors for significantly intense reflections: 0.1247
• Weighted residual factors for all reflections included in the refinement: 0.131
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No