Information card for entry 7705700

Structure parameters

• Formula: C97 H204 K4 O24 Si16
• Calculated formula: C97 H204 K4 O24 Si16
• Title of publication: Long-range coupling in cyclic silanes.
• Authors of publication: Ferguson, John T.; Jiang, Qifeng; Marro, Eric A.; Siegler, Maxime A.; Klausen, Rebekka S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 42
• Pages of publication: 14951 - 14961
• a: 13.3319 ± 0.0003 Å
• b: 21.5603 ± 0.0005 Å
• c: 23.7767 ± 0.0006 Å
• α: 90°
• β: 99.786 ± 0.002°
• γ: 90°
• Cell volume: 6734.9 ± 0.3 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0643
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.1033
• Weighted residual factors for all reflections included in the refinement: 0.1101
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No