Information card for entry 7705775

Structure parameters

• Formula: C18 H18 As Br2 Co N3
• Calculated formula: C18 H18 As Br2 Co N3
• Title of publication: Coordination chemistry of the bench-stable tris-2-pyridyl pnictogen ligands [E(6-Me-2-py)₃] (E = As, As[double bond, length as m-dash]O, Sb).
• Authors of publication: Plajer, Alex J.; Crusius, Daniel; Jethwa, Rajesh B.; García-Romero, Álvaro; Bond, Andrew D.; García-Rodríguez, Raúl; Wright, Dominic S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 7
• Pages of publication: 2393 - 2402
• a: 8.2686 ± 0.0002 Å
• b: 8.6144 ± 0.0003 Å
• c: 15.8017 ± 0.0005 Å
• α: 101.168 ± 0.0015°
• β: 93.4356 ± 0.0014°
• γ: 115.304 ± 0.0013°
• Cell volume: 985.27 ± 0.05 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0327
• Residual factor for significantly intense reflections: 0.0265
• Weighted residual factors for significantly intense reflections: 0.0608
• Weighted residual factors for all reflections included in the refinement: 0.0633
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No