Crystallography Open Database

Information card for entry 7705852

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Coordinates	7705852.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C73 H85 B F24 N P2 Rh
Calculated formula	C73 H85 B F24 N P2 Rh
Title of publication	Reactions of Rh(PNP) pincer complexes with terminal alkynes: homocoupling through a ring or not at all.
Authors of publication	Hood, Thomas M.; Chaplin, Adrian B.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	46
Pages of publication	16649 - 16652
a	18.53479 ± 0.00012 Å
b	20.42808 ± 0.00012 Å
c	40.2348 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	15234.1 ± 0.18 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0743
Residual factor for significantly intense reflections	0.0679
Weighted residual factors for significantly intense reflections	0.1778
Weighted residual factors for all reflections included in the refinement	0.1871
Goodness-of-fit parameter for all reflections included in the refinement	1.025
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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