Information card for entry 7705855

Structure parameters

• Formula: C71 H81 B F24 N O2 P2 Rh
• Calculated formula: C71 H81 B F24 N O2 P2 Rh
• Title of publication: Reactions of Rh(PNP) pincer complexes with terminal alkynes: homocoupling through a ring or not at all.
• Authors of publication: Hood, Thomas M.; Chaplin, Adrian B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 46
• Pages of publication: 16649 - 16652
• a: 26.2257 ± 0.0001 Å
• b: 18.1905 ± 0.0001 Å
• c: 15.8286 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7551.17 ± 0.07 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.034
• Residual factor for significantly intense reflections: 0.0323
• Weighted residual factors for significantly intense reflections: 0.0864
• Weighted residual factors for all reflections included in the refinement: 0.0881
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No