Information card for entry 7705858

Structure parameters

• Chemical name: (chloro)(chlorosilyl)cyclotrisilene-DMAP
• Formula: C51 H102 Cl2 N2 Si12
• Calculated formula: C51 H102 Cl2 N2 Si12
• Title of publication: Interconversion between a planar 1,3-dichlorobicyclo[1.1.0]tetrasilane and a (chloro)(chlorosilyl)cyclotrisilene.
• Authors of publication: Nukazawa, Takumi; Iwamoto, Takeaki
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 46
• Pages of publication: 16728 - 16735
• a: 13.5086 ± 0.0003 Å
• b: 15.0599 ± 0.0004 Å
• c: 16.6833 ± 0.0004 Å
• α: 89.364 ± 0.001°
• β: 85.209 ± 0.001°
• γ: 76.743 ± 0.001°
• Cell volume: 3291.92 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0521
• Residual factor for significantly intense reflections: 0.0356
• Weighted residual factors for significantly intense reflections: 0.0802
• Weighted residual factors for all reflections included in the refinement: 0.0887
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No