Information card for entry 7706166

Structure parameters

• Formula: F4 K4 O11 P2 S2
• Calculated formula: F4 K4 O11 P2 S2
• Title of publication: K₄(PO₂F₂)₂(S₂O₇): first fluorooxophosphorsulfate with mixed-anion [S₂O₇]^2- and [PO₂F₂]^- groups.
• Authors of publication: Zhang, Wenyao; Jin, Wenqi; Yang, Zhihua; Pan, Shilie
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 48
• Pages of publication: 17658 - 17664
• a: 13 ± 0.001 Å
• b: 7.543 ± 0.001 Å
• c: 19.01 ± 0.0001 Å
• α: 90°
• β: 130.07 ± 0.001°
• γ: 90°
• Cell volume: 1426.5 ± 0.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0784
• Residual factor for significantly intense reflections: 0.0471
• Weighted residual factors for significantly intense reflections: 0.0732
• Weighted residual factors for all reflections included in the refinement: 0.0812
• Goodness-of-fit parameter for all reflections included in the refinement: 1.125
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No