Information card for entry 7706300

Structure parameters

• Formula: C37 H29 O12 S3 W2
• Calculated formula: C37 H29 O12 S3 W2
• Title of publication: Chelated Fischer carbene complexes of annulated thiophenes: synthesis, structure and electrochemistry.
• Authors of publication: Lamprecht, Zandria; Malan, Frederick P.; Fernández, Israel; Lotz, Simon; Bezuidenhout, Daniela I.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 43
• Pages of publication: 15339 - 15354
• a: 11.0377 ± 0.0011 Å
• b: 12.018 ± 0.0011 Å
• c: 16.5239 ± 0.0016 Å
• α: 69.06 ± 0.003°
• β: 74.437 ± 0.003°
• γ: 77.654 ± 0.003°
• Cell volume: 1955.1 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0334
• Residual factor for significantly intense reflections: 0.0289
• Weighted residual factors for significantly intense reflections: 0.0757
• Weighted residual factors for all reflections included in the refinement: 0.078
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No