Information card for entry 7706446

Structure parameters

• Formula: C63 H53 B Bi Cl2 F15 N2
• Calculated formula: C63 H53 B Bi Cl2 F15 N2
• Title of publication: Stabilization of a bismuth-bismuth double bond by anionic N-heterocyclic carbenes.
• Authors of publication: Ho, Luong Phong; Tamm, Matthias
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 4
• Pages of publication: 1202 - 1205
• a: 15.9856 ± 0.0004 Å
• b: 12.4306 ± 0.0002 Å
• c: 29.7067 ± 0.0006 Å
• α: 90°
• β: 97.483 ± 0.002°
• γ: 90°
• Cell volume: 5852.8 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0557
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for significantly intense reflections: 0.1108
• Weighted residual factors for all reflections included in the refinement: 0.1126
• Goodness-of-fit parameter for all reflections included in the refinement: 1.242
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No