Information card for entry 7706506

Structure parameters

• Formula: Cs10 H29 Na2 Ni4 O98 Si2 W20
• Calculated formula: Cs10 Na2 Ni4 O98 Si2 W20
• Title of publication: Synthesis, structure, electrochemistry and magnetism of cobalt-, nickel- and zinc-containing [M₄(OH)₃(H₂O)₂(α-SiW₁₀O_36.5)₂]^13- (M = Co²⁺, Ni²⁺, and Zn²⁺).
• Authors of publication: Haider, Ali; Bassil, Bassem S.; Lin, Zhengguo; Ma, Xiang; Haferl, Peter J.; Bindra, Jasleen K.; Kinyon, Jared; Zhang, Guangjin; Keita, Bineta; Dalal, Naresh S.; Kortz, Ulrich
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 11
• Pages of publication: 3923 - 3930
• a: 13.0666 ± 0.0005 Å
• b: 15.6924 ± 0.0006 Å
• c: 23.7612 ± 0.0009 Å
• α: 90°
• β: 100.454 ± 0.003°
• γ: 90°
• Cell volume: 4791.3 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0903
• Residual factor for significantly intense reflections: 0.0531
• Weighted residual factors for significantly intense reflections: 0.1266
• Weighted residual factors for all reflections included in the refinement: 0.1438
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No