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Information card for entry 7706516
Preview
Coordinates | 7706516.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C4 H20 B18 Co Cs I2 |
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Calculated formula | C4 H20 B18 Co Cs I2 |
Title of publication | The unexpected reactivity of 9-iodo-nido-carborane: from nucleophilic substitution reactions to the synthesis of tricobalt tris(dicarbollide) Na[4,4',4''-(MeOCH<sub>2</sub>CH<sub>2</sub>O)<sub>3</sub>-3,3',3''-Co<sub>3</sub>(μ<sup>3</sup>-O)(μ<sup>3</sup>-S)(1,2-C<sub>2</sub>B<sub>9</sub>H<sub>10</sub>)<sub>3</sub>]. |
Authors of publication | Stogniy, Marina Yu; Anufriev, Sergey A.; Shmal'ko, Akim V.; Antropov, Sergey M.; Anisimov, Aleksei A.; Suponitsky, Kyrill Yu; Filippov, Oleg A.; Sivaev, Igor B. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2021 |
Journal volume | 50 |
Journal issue | 7 |
Pages of publication | 2671 - 2688 |
a | 8.7703 ± 0.0006 Å |
b | 10.6041 ± 0.0006 Å |
c | 12.3092 ± 0.0007 Å |
α | 71.445 ± 0.001° |
β | 85.935 ± 0.001° |
γ | 73.426 ± 0.001° |
Cell volume | 1039.92 ± 0.11 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0153 |
Residual factor for significantly intense reflections | 0.0141 |
Weighted residual factors for significantly intense reflections | 0.0319 |
Weighted residual factors for all reflections included in the refinement | 0.0323 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.129 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7706516.html
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Users of the data should acknowledge the original authors of the
structural data.