Information card for entry 7706540

Structure parameters

• Formula: C27 H36 Al Cl3 N2
• Calculated formula: C27 H36 Al Cl3 N2
• Title of publication: The carbene transfer to strong Lewis acids: copper is better than silver.
• Authors of publication: Mikhaylov, Vladimir N.; Kazakov, Igor V.; Parfeniuk, Tatiana N.; Khoroshilova, Olesya V.; Scheer, Manfred; Timoshkin, Alexey Y.; Balova, Irina A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 8
• Pages of publication: 2872 - 2879
• a: 16.49269 ± 0.00012 Å
• b: 19.41043 ± 0.00012 Å
• c: 19.28026 ± 0.00014 Å
• α: 90°
• β: 112.261 ± 0.0009°
• γ: 90°
• Cell volume: 5712.15 ± 0.08 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0385
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0891
• Weighted residual factors for all reflections included in the refinement: 0.0915
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No