Information card for entry 7706542

Structure parameters

• Formula: C54 H72 Ag Al Cl4 N4
• Calculated formula: C54 H72 Ag Al Cl4 N4
• Title of publication: The carbene transfer to strong Lewis acids: copper is better than silver.
• Authors of publication: Mikhaylov, Vladimir N.; Kazakov, Igor V.; Parfeniuk, Tatiana N.; Khoroshilova, Olesya V.; Scheer, Manfred; Timoshkin, Alexey Y.; Balova, Irina A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 8
• Pages of publication: 2872 - 2879
• a: 17.0566 ± 0.0002 Å
• b: 18.1442 ± 0.0002 Å
• c: 18.0974 ± 0.0002 Å
• α: 90°
• β: 100.508 ± 0.001°
• γ: 90°
• Cell volume: 5506.83 ± 0.11 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0329
• Residual factor for significantly intense reflections: 0.0322
• Weighted residual factors for significantly intense reflections: 0.0801
• Weighted residual factors for all reflections included in the refinement: 0.0807
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No