Information card for entry 7706603

Structure parameters

• Formula: C33 H33 N2 O4 P Pd S
• Calculated formula: C33 H33 N2 O4 P Pd S
• Title of publication: Controlled di-lithiation enabled synthesis of phosphine-sulfonamide ligands and implications in ethylene oligomerization.
• Authors of publication: Mote, Nilesh R.; Gaikwad, Shahaji R.; Khopade, Kishor V.; Gonnade, Rajesh G.; Chikkali, Samir H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 10
• Pages of publication: 3717 - 3723
• a: 12.3236 ± 0.0013 Å
• b: 18.867 ± 0.002 Å
• c: 13.3975 ± 0.0015 Å
• α: 90°
• β: 105.039 ± 0.004°
• γ: 90°
• Cell volume: 3008.4 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0274
• Residual factor for significantly intense reflections: 0.0237
• Weighted residual factors for significantly intense reflections: 0.0568
• Weighted residual factors for all reflections included in the refinement: 0.0605
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No