Information card for entry 7706623

Structure parameters

• Formula: C106 H126 B3 F30 P3
• Calculated formula: C106 H126 B3 F30 P3
• Title of publication: Reaction of carbon oxides with an ethylene-bridged PH/B Lewis pair.
• Authors of publication: Sun, Qiu; Daniliuc, Constantin G.; Kehr, Gerald; Erker, Gerhard
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 10
• Pages of publication: 3523 - 3528
• a: 13.8401 ± 0.0003 Å
• b: 19.2176 ± 0.0005 Å
• c: 19.5735 ± 0.0005 Å
• α: 84.129 ± 0.002°
• β: 85.038 ± 0.002°
• γ: 85.211 ± 0.002°
• Cell volume: 5144.7 ± 0.2 ų
• Cell temperature: 446 ± 2 K
• Ambient diffraction temperature: 446 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1081
• Residual factor for significantly intense reflections: 0.0614
• Weighted residual factors for significantly intense reflections: 0.1454
• Weighted residual factors for all reflections included in the refinement: 0.1736
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No