Information card for entry 7706629

Structure parameters

• Formula: C55 H52 B2 F20 N O P
• Calculated formula: C55 H52 B2 F20 N O P
• Title of publication: Reaction of carbon oxides with an ethylene-bridged PH/B Lewis pair.
• Authors of publication: Sun, Qiu; Daniliuc, Constantin G.; Kehr, Gerald; Erker, Gerhard
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 10
• Pages of publication: 3523 - 3528
• a: 12.4179 ± 0.0005 Å
• b: 15.1109 ± 0.0006 Å
• c: 17.2639 ± 0.0006 Å
• α: 112.91 ± 0.001°
• β: 99.423 ± 0.001°
• γ: 106.422 ± 0.001°
• Cell volume: 2721.35 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0737
• Residual factor for significantly intense reflections: 0.0429
• Weighted residual factors for significantly intense reflections: 0.0974
• Weighted residual factors for all reflections included in the refinement: 0.1144
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No