Crystallography Open Database

Information card for entry 7706636

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Coordinates	7706636.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H48 B2 O6 Rh2
Calculated formula	C28 H48 B2 O6 Rh2
Title of publication	Synthesis and reactivity of boryloxorhodium complexes. Relevance to intermolecular transmetalation from boron to rhodium in Rh-catalyzed reactions.
Authors of publication	Nishihara, Yasushi; Nishide, Yasuhiro; Osakada, Kohtaro
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	10
Pages of publication	3610 - 3615
a	22.997 ± 0.005 Å
b	6.3442 ± 0.0013 Å
c	20.881 ± 0.006 Å
α	90°
β	95.251°
γ	90°
Cell volume	3033.7 ± 1.3 Å³
Cell temperature	296 K
Ambient diffraction temperature	296 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.031
Weighted residual factors for all reflections included in the refinement	0.0939
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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