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Information card for entry 7706638
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Coordinates | 7706638.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C37.6 H36 P Rh |
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Calculated formula | C37.6 H36 P Rh |
Title of publication | Synthesis and reactivity of boryloxorhodium complexes. Relevance to intermolecular transmetalation from boron to rhodium in Rh-catalyzed reactions. |
Authors of publication | Nishihara, Yasushi; Nishide, Yasuhiro; Osakada, Kohtaro |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2021 |
Journal volume | 50 |
Journal issue | 10 |
Pages of publication | 3610 - 3615 |
a | 10.443 ± 0.003 Å |
b | 22.412 ± 0.003 Å |
c | 14.037 ± 0.003 Å |
α | 90° |
β | 102.93° |
γ | 90° |
Cell volume | 3202 ± 1.2 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0716 |
Residual factor for significantly intense reflections | 0.0371 |
Weighted residual factors for significantly intense reflections | 0.0919 |
Weighted residual factors for all reflections included in the refinement | 0.1062 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.008 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7706638.html
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structural data.