Information card for entry 7706756

Structure parameters

• Formula: C193.59 H419.17 Hf2 N6 O85.39 P2 Si6 W18
• Calculated formula: C193.62 H419.238 Hf2 N6 O85.402 P2 Si6 W18
• Title of publication: Development of sterically hindered siloxide-functionalized polyoxotungstates for the complexation of 5d-metals.
• Authors of publication: Auvray, Thomas; Nachtigall, Olaf; Brennessel, William W.; Jones, William D.; Matson, Ellen M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 12
• Pages of publication: 4300 - 4310
• a: 25.2799 ± 0.0003 Å
• b: 25.724 ± 0.0003 Å
• c: 21.8787 ± 0.0003 Å
• α: 90°
• β: 99.683 ± 0.001°
• γ: 90°
• Cell volume: 14025 ± 0.3 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0718
• Residual factor for significantly intense reflections: 0.0645
• Weighted residual factors for significantly intense reflections: 0.1808
• Weighted residual factors for all reflections included in the refinement: 0.1882
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No