Information card for entry 7706808

Structure parameters

• Formula: C47 H65 N O Pb
• Calculated formula: C47 H65 N O Pb
• Title of publication: Low valent lead and tin hydrides in reactions with heteroallenes.
• Authors of publication: Weiß, Sebastian; Widemann, Max; Eichele, Klaus; Schubert, Hartmut; Wesemann, Lars
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 14
• Pages of publication: 4952 - 4958
• a: 19.0155 ± 0.0007 Å
• b: 18.4067 ± 0.0007 Å
• c: 12.1142 ± 0.0004 Å
• α: 90°
• β: 99.691 ± 0.002°
• γ: 90°
• Cell volume: 4179.6 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0829
• Residual factor for significantly intense reflections: 0.0693
• Weighted residual factors for significantly intense reflections: 0.1587
• Weighted residual factors for all reflections included in the refinement: 0.1628
• Goodness-of-fit parameter for all reflections included in the refinement: 1.295
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No