Information card for entry 7706857

Structure parameters

• Common name: 6-chloro-1,4-dimethyl-10H-5,10-[1,2]benzenoacridophosphine
• Chemical name: 6-chloro-1,4-dimethyl-10H-5,10-[1,2]benzenoacridophosphine
• Formula: C21 H16 Cl P
• Calculated formula: C21 H16 Cl P
• Title of publication: Sterically hindered ortho-substituted phosphatriptycenes as configurationally stable P-chirogenic triarylphosphines.
• Authors of publication: Hu, Lei; Mahaut, Damien; Tumanov, Nikolay; Wouters, Johan; Collard, Laurent; Robiette, Raphaël; Berionni, Guillaume
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 14
• Pages of publication: 4772 - 4777
• a: 13.987 ± 0.0017 Å
• b: 16.009 ± 0.004 Å
• c: 16.436 ± 0.004 Å
• α: 74.36 ± 0.02°
• β: 89.257 ± 0.014°
• γ: 79.319 ± 0.016°
• Cell volume: 3480 ± 1.3 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1586
• Residual factor for significantly intense reflections: 0.0877
• Weighted residual factors for significantly intense reflections: 0.1992
• Weighted residual factors for all reflections included in the refinement: 0.2354
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No