Information card for entry 7706912

Structure parameters

• Formula: C42 H76 Cr K N2 Si2
• Calculated formula: C42 H76 Cr K N2 Si2
• Title of publication: Quasilinear 3d-metal(i) complexes [KM(N(Dipp)SiR₃)₂] (M = Cr-Co) - structural diversity, solution state behaviour and reactivity.
• Authors of publication: Weller, Ruth; Müller, Igor; Duhayon, Carine; Sabo-Etienne, Sylviane; Bontemps, Sébastien; Werncke, C. Gunnar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 14
• Pages of publication: 4890 - 4903
• a: 22.775 ± 0.0014 Å
• b: 22.3023 ± 0.0013 Å
• c: 17.1996 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8736.3 ± 0.9 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 99.99 K
• Number of distinct elements: 6
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0895
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for significantly intense reflections: 0.1031
• Weighted residual factors for all reflections included in the refinement: 0.1112
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No