Information card for entry 7706922

Structure parameters

• Formula: C46 H84 Fe Li N2 O8 Si2
• Calculated formula: C46 H84 Fe Li N2 O8 Si2
• Title of publication: Quasilinear 3d-metal(i) complexes [KM(N(Dipp)SiR₃)₂] (M = Cr-Co) - structural diversity, solution state behaviour and reactivity.
• Authors of publication: Weller, Ruth; Müller, Igor; Duhayon, Carine; Sabo-Etienne, Sylviane; Bontemps, Sébastien; Werncke, C. Gunnar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 14
• Pages of publication: 4890 - 4903
• a: 11.6888 ± 0.0008 Å
• b: 14.5127 ± 0.001 Å
• c: 16.4126 ± 0.0012 Å
• α: 70.55 ± 0.002°
• β: 83.481 ± 0.002°
• γ: 77.315 ± 0.002°
• Cell volume: 2558.7 ± 0.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0979
• Residual factor for significantly intense reflections: 0.0826
• Weighted residual factors for significantly intense reflections: 0.1912
• Weighted residual factors for all reflections included in the refinement: 0.1996
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No