Information card for entry 7706925

Structure parameters

• Formula: C60 H50 Fe K O
• Calculated formula: C60 H50 Fe K O
• Title of publication: Quasilinear 3d-metal(i) complexes [KM(N(Dipp)SiR₃)₂] (M = Cr-Co) - structural diversity, solution state behaviour and reactivity.
• Authors of publication: Weller, Ruth; Müller, Igor; Duhayon, Carine; Sabo-Etienne, Sylviane; Bontemps, Sébastien; Werncke, C. Gunnar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 14
• Pages of publication: 4890 - 4903
• a: 19.3467 ± 0.0007 Å
• b: 11.2945 ± 0.0004 Å
• c: 21.4705 ± 0.0009 Å
• α: 90°
• β: 102.473 ± 0.0013°
• γ: 90°
• Cell volume: 4580.8 ± 0.3 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.047
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for significantly intense reflections: 0.087
• Weighted residual factors for all reflections included in the refinement: 0.092
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No