Crystallography Open Database

Information card for entry 7707034

Preview

Coordinates	7707034.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H48 Li4 N12
Calculated formula	C48 H48 Li4 N12
Title of publication	Coordination capabilities of bis-(2-pyridyl)amides in the field of divalent germanium, tin and lead compounds.
Authors of publication	Zechovský, Jan; Mrózek, Ondřej; Samsonov, Maksim; Jambor, Roman; RůŽička, Aleš; Dostál, Libor
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	18
Pages of publication	6321 - 6332
a	11.1572 ± 0.0004 Å
b	11.5648 ± 0.0004 Å
c	19.6657 ± 0.0007 Å
α	79.294 ± 0.002°
β	76.67 ± 0.002°
γ	62.192 ± 0.002°
Cell volume	2174.94 ± 0.14 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2008
Residual factor for significantly intense reflections	0.1095
Weighted residual factors for significantly intense reflections	0.2443
Weighted residual factors for all reflections included in the refinement	0.2939
Goodness-of-fit parameter for all reflections included in the refinement	1.297
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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