Information card for entry 7707189

Structure parameters

• Formula: C30 H30 Na4.55 Nb12 O64.25 Ru5 V
• Calculated formula: C30 H30 Na4.55 Nb12 O64.25 Ru5 V
• Title of publication: Coordination capacity of Keggin anions as polytopic ligands: case study of [VNb₁₂O₄₀]¹⁵.
• Authors of publication: Mukhacheva, Anna A.; Volcheck, Victoria V.; Sheven, Dmitry G.; Yanshole, Vadim V.; Kompankov, Nikolay B.; Haouas, Mohamed; Abramov, Pavel A.; Sokolov, Maxim N.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 20
• Pages of publication: 7078 - 7084
• a: 14.1141 ± 0.0007 Å
• b: 16.3111 ± 0.001 Å
• c: 22.4722 ± 0.0009 Å
• α: 92.167 ± 0.004°
• β: 93.075 ± 0.004°
• γ: 114.998 ± 0.005°
• Cell volume: 4671.6 ± 0.5 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1746
• Residual factor for significantly intense reflections: 0.0784
• Weighted residual factors for significantly intense reflections: 0.1625
• Weighted residual factors for all reflections included in the refinement: 0.1928
• Goodness-of-fit parameter for all reflections included in the refinement: 0.942
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No