Information card for entry 7707201

Structure parameters

• Formula: C42 H44 Cu4 K N14 Nb9 O42 Te V2
• Calculated formula: C42 H44 Cu4 K N14 Nb9 O42 Te V2
• Title of publication: Synthesis, structures and stability of three V-substituted polyoxoniobate clusters based on [TeNb₉O₃₃]^17- units.
• Authors of publication: Yang, Zongfei; Shang, Jingjing; Yang, Yuanyuan; Ma, Pengtao; Niu, Jingyang; Wang, Jingping
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 22
• Pages of publication: 7610 - 7620
• a: 15.4162 ± 0.0015 Å
• b: 18.938 ± 0.0017 Å
• c: 21.0858 ± 0.0019 Å
• α: 63.501 ± 0.002°
• β: 71.908 ± 0.003°
• γ: 84.15 ± 0.003°
• Cell volume: 5232.1 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 149.98 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1415
• Residual factor for significantly intense reflections: 0.0694
• Weighted residual factors for significantly intense reflections: 0.1633
• Weighted residual factors for all reflections included in the refinement: 0.2055
• Goodness-of-fit parameter for all reflections included in the refinement: 0.985
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No