Information card for entry 7707233

Structure parameters

• Formula: C126 H162 B4 K4 N8 O8
• Calculated formula: C126 H162 B4 K4 N8 O8
• Title of publication: Reactions of a diborylstannylene with CO₂ and N₂O: diboration of carbon dioxide by a main group bis(boryl) complex.
• Authors of publication: Protchenko, Andrey V.; Fuentes, M Ángeles; Hicks, Jamie; McManus, Caitilín; Tirfoin, Rémi; Aldridge, Simon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 26
• Pages of publication: 9059 - 9067
• a: 29.0119 ± 0.0002 Å
• b: 15.7055 ± 0.0001 Å
• c: 28.1694 ± 0.0003 Å
• α: 90°
• β: 103.568 ± 0.001°
• γ: 90°
• Cell volume: 12477.1 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0729
• Residual factor for significantly intense reflections: 0.0654
• Weighted residual factors for significantly intense reflections: 0.1996
• Weighted residual factors for all reflections included in the refinement: 0.21
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No