Information card for entry 7707235

Structure parameters

• Formula: C58 H80 B2 Br Li N4 O5 Sn
• Calculated formula: C58 H80 B2 Br Li N4 O5 Sn
• Title of publication: Reactions of a diborylstannylene with CO₂ and N₂O: diboration of carbon dioxide by a main group bis(boryl) complex.
• Authors of publication: Protchenko, Andrey V.; Fuentes, M Ángeles; Hicks, Jamie; McManus, Caitilín; Tirfoin, Rémi; Aldridge, Simon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 26
• Pages of publication: 9059 - 9067
• a: 10.341 ± 0.0001 Å
• b: 21.4584 ± 0.0001 Å
• c: 27.4349 ± 0.0001 Å
• α: 90°
• β: 92.851 ± 0.001°
• γ: 90°
• Cell volume: 6080.31 ± 0.07 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0367
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for significantly intense reflections: 0.0867
• Weighted residual factors for all reflections included in the refinement: 0.0887
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No