Information card for entry 7707237

Structure parameters

• Formula: C64 H89 B2 N6 O4 Sn
• Calculated formula: C64 H89 B2 N6 O4 Sn
• Title of publication: Reactions of a diborylstannylene with CO₂ and N₂O: diboration of carbon dioxide by a main group bis(boryl) complex.
• Authors of publication: Protchenko, Andrey V.; Fuentes, M Ángeles; Hicks, Jamie; McManus, Caitilín; Tirfoin, Rémi; Aldridge, Simon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 26
• Pages of publication: 9059 - 9067
• a: 9.9561 ± 0.0001 Å
• b: 22.1784 ± 0.0003 Å
• c: 29.1176 ± 0.0003 Å
• α: 90°
• β: 97.887 ± 0.001°
• γ: 90°
• Cell volume: 6368.65 ± 0.13 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0506
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.1084
• Weighted residual factors for all reflections included in the refinement: 0.1156
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No