Information card for entry 7707239

Structure parameters

• Formula: C108 H144 B4 N8 O9 Sn3
• Calculated formula: C108 H144 B4 N8 O9 Sn3
• Title of publication: Reactions of a diborylstannylene with CO₂ and N₂O: diboration of carbon dioxide by a main group bis(boryl) complex.
• Authors of publication: Protchenko, Andrey V.; Fuentes, M Ángeles; Hicks, Jamie; McManus, Caitilín; Tirfoin, Rémi; Aldridge, Simon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 26
• Pages of publication: 9059 - 9067
• a: 14.3697 ± 0.0003 Å
• b: 14.8194 ± 0.0003 Å
• c: 28.2627 ± 0.0006 Å
• α: 77.969 ± 0.002°
• β: 78.949 ± 0.002°
• γ: 67.294 ± 0.002°
• Cell volume: 5388.7 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0362
• Residual factor for significantly intense reflections: 0.0307
• Weighted residual factors for significantly intense reflections: 0.0757
• Weighted residual factors for all reflections included in the refinement: 0.079
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No