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Information card for entry 7707404
Preview
Coordinates | 7707404.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C29 H51 Cl O P U |
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Calculated formula | C29 H51 Cl O P U |
Title of publication | Reactivity studies involving a Lewis base supported terminal uranium phosphinidene metallocene [η<sup>5</sup>-1,3-(Me<sub>3</sub>C)<sub>2</sub>C<sub>5</sub>H<sub>3</sub>]<sub>2</sub>U([double bond, length as m-dash]P-2,4,6-<sup>i</sup>Pr<sub>3</sub>C<sub>6</sub>H<sub>2</sub>)(OPMe<sub>3</sub>). |
Authors of publication | Wang, Deqiang; Wang, Shichun; Li, Tongyu; Heng, Yi; Hou, Guohua; Zi, Guofu; Walter, Marc D. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2021 |
Journal volume | 50 |
Journal issue | 24 |
Pages of publication | 8349 - 8363 |
a | 10.3013 ± 0.0001 Å |
b | 11.9655 ± 0.0002 Å |
c | 29.1545 ± 0.0004 Å |
α | 90° |
β | 90.581 ± 0.001° |
γ | 90° |
Cell volume | 3593.4 ± 0.09 Å3 |
Cell temperature | 100.02 ± 0.1 K |
Ambient diffraction temperature | 100.02 ± 0.1 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0298 |
Residual factor for significantly intense reflections | 0.0284 |
Weighted residual factors for significantly intense reflections | 0.0717 |
Weighted residual factors for all reflections included in the refinement | 0.0729 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.045 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7707404.html
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