Information card for entry 7707461

Structure parameters

• Formula: C34 H51 N3 Si2
• Calculated formula: C34 H51 N3 Si2
• Title of publication: Imino(silyl)disilenes: application in versatile bond activation, reversible oxidation and thermal isomerization.
• Authors of publication: Holzner, Richard; Porzelt, Amelie; Karaca, Uhut S.; Kiefer, Fiona; Frisch, Philipp; Wendel, Daniel; Holthausen, Max C.; Inoue, Shigeyoshi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 25
• Pages of publication: 8785 - 8793
• a: 10.1287 ± 0.0011 Å
• b: 19.437 ± 0.002 Å
• c: 16.5735 ± 0.0018 Å
• α: 90°
• β: 95.309 ± 0.004°
• γ: 90°
• Cell volume: 3248.9 ± 0.6 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0447
• Residual factor for significantly intense reflections: 0.0404
• Weighted residual factors for significantly intense reflections: 0.1
• Weighted residual factors for all reflections included in the refinement: 0.1026
• Goodness-of-fit parameter for all reflections included in the refinement: 1.122
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No