Information card for entry 7707498

Structure parameters

• Formula: C50 H66 Al2 D12 N4
• Calculated formula: C50 H66 Al2 D12 N4
• Title of publication: Synthesis, characterization, and reactivity of group 13 hydride complexes based on amido-amine ligands.
• Authors of publication: Dehmel, Maximilian; Köhler, Angelina; Görls, Helmar; Kretschmer, Robert
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 24
• Pages of publication: 8434 - 8445
• a: 10.8556 ± 0.0004 Å
• b: 11.7894 ± 0.0004 Å
• c: 11.8812 ± 0.0005 Å
• α: 62.401 ± 0.004°
• β: 66.258 ± 0.004°
• γ: 67.286 ± 0.003°
• Cell volume: 1195.57 ± 0.09 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0497
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for significantly intense reflections: 0.115
• Weighted residual factors for all reflections included in the refinement: 0.1211
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No