Information card for entry 7707569

Structure parameters

• Formula: C53 H77 N3 Pb Si2
• Calculated formula: C53 H77 N3 Pb Si2
• Title of publication: Bis(imino)carbazolate lead(II) fluoride and related halides.
• Authors of publication: Chapple, Peter M.; Hamdoun, Ghanem; Roisnel, Thierry; Carpentier, Jean-François; Oulyadi, Hassan; Sarazin, Yann
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 26
• Pages of publication: 9021 - 9025
• a: 12.863 ± 0.004 Å
• b: 13.581 ± 0.005 Å
• c: 16.539 ± 0.006 Å
• α: 70.105 ± 0.011°
• β: 79.2 ± 0.012°
• γ: 76.778 ± 0.009°
• Cell volume: 2625.8 ± 1.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0665
• Residual factor for significantly intense reflections: 0.0471
• Weighted residual factors for significantly intense reflections: 0.1012
• Weighted residual factors for all reflections included in the refinement: 0.11
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No